Numune Hazırlama
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0.45 mikron RC filtreden filtre karışımı, doğrudan sisteme enjekte edin.
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Filter mixture from 0.45 micron RC filter, Directly inject into the system.
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Numune üzerine 60 µl ISTD çözeltisi ve 2.0 ml Reaktif-1 ekleyin ve 30 saniye vorteksleyin.
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5 dakika boyunca 3000 rpm'de santrifüjleyin.
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Antibiyotiklerin toplam iyon kromatogramı
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Sütte Çoklu Antibiyotik Kitinin Antibiyotik Listesi
Antibiyotikler
LOQ
(µg/kg)
Geri Kazanım
(%)
RSD
(%)
1
5-hyroxy thiobendazole
0.47
99
1.49
2
Abamectin
0.84
101
9.39
3
Albendazole
0.12
106
1.59
4
Ampicillin
0.78
101
5.50
5
Amoxicillin
0.33
102
1.91
6
Ciprofloxacin
0.40
100
1.54
7
Danofloxacin
0.26
97
0.94
8
Difloxacin
0.25
106
1.98
9
Doxycycline
0.51
64
7.08
10
Doramectin
0.95
108
4.74
11
Enrofloxacin
0.29
103
1.21
12
Epinomectin
0.55
98
8.03
13
Erythromycin
0.45
104
4.14
14
Fenbendazole
0.10
107
1.74
15
Flumequine
0.12
104
2.03
16
Ipronidazole
0.68
97
1.75
17
Ipronidazole-hydroxy
1.06
88
7.84
18
Ivermectin
0.58
98
5.91
19
Chlortetracycline
4.29
102
5.26
20
Levamisole HCl
0.22
115
1.40
21
Marbofloxacin
0.15
110
1.19
22
Mebendazole
0.28
103
1.87
23
Metronidazole
0.78
97
2.28
24
Moxidectin
0.55
96
4.52
25
Nalidixic acid
0.16
108
2.19
26
Naracin
0.09
102
4.59
27
Oxacillin
3.67
108
4.96
28
Oxytetracycline
0.86
109
4.73
29
Oxfendazole
0.34
98
1.42
30
Oxolinic acid
0.16
112
1.58
31
Penicillin G
0.32
102
1.93
32
Ronidazole
0.96
98
2.52
33
Salinomcysin
0.10
102
7.25
34
Sarafloxacin
0.52
97
2.09
35
Sulfadiazin
0.32
95
3.08
36
Sulfadimethoxin
0.56
101
1.58
37
Sulfadioxin
0.29
100
2.06
38
Sulfachloropyridazine
1.48
89
6.12
39
Sulfamerazin
0.44
101
1.36
40
Sulfametoxazole
0.95
73
3.70
41
Sulfamethazine
0.54
97
1.96
42
Sulfathiazole
0.79
96
1.65
43
Sulfapyrdine
0.39
112
2.48
44
Sulfaquinoxaline
0.58
104
2.24
45
Tetracycline
1.04
98
5.30
46
Thiabendazole
0.34
86
3.50
47
Tilmicosin
0.48
111
1.70
48
Tylosin
0.70
107
1.71
49
Triclabendazole
0.83
108
4.43
50
Toltrazural
0.11
102
4.08